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The recent applications of in situ Raman and X-ray absorption spectroscopies for various energy-related electrochemical reactions occurring on nano- and single-atom catalysts are summarized. Using these techniques, the oxygen-containing intermediate species are captured during the reduction of oxygen and the oxidation of hydrogen, and the structural transformation of catalysts with the change of potentials is detected during the evolution of oxygen and reduction of CO2.
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Chinese Journal of Catalysis
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